Al_2O_3-Coated Nano-SiC Particles Reinforced Al_2O_3 Matrix Composites

来源 :Journal of Materials Science & Technology | 被引量 : 0次 | 上传用户:wzlzcy_yt190057
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Properties of Al2O3-coated nano-SiC have been compared with those of as-received SiC. The isoelectric point (IEP) of SiC changed from pH3.4 to pH7.3 after coating with the alumina precursor, which is close to that of alumina. Because both surfaces of coated SiC and AI2O3 possess higher positive charge at pH=4.5-5.0, they are uniformly dispersed in the two-phase aqueous suspensions, Then a mixed powder containing nano-SiC dispersed homogeneously into the Al2O3 matrix was achieved from flocculating the two-phase suspension. Finally, Al2O3/SiC nanocomposites were obtained by coating nano-SiC with Al2O3, in which the majority of SiC particles were located within the AI2O3 grains. The observation by transmission electron microscopy (TEM) and the analysis by the X-ray photoelectron spectroscopy (XPS) showed that cracks propagated towards the intragranular SiC rather than along grain boundaries. The properties of Al2O3-coated nano-SiC have been compared with those of as-received SiC. The isoelectric point (IEP) of SiC changed from pH 3.4 to pH 7.3 after coating with the alumina precursor, which is close to that of alumina . Both of the surfaces of coated SiC and AI2O3 possess higher positive charge at pH = 4.5-5.0, they are dispersed dispersed in the two-phase aqueous suspensions, then a mixed powder containing nano-SiC dispersed homogeneously into the Al2O3 matrix was achieved from flocculating the two-phase suspension. Finally, Al2O3 / SiC nanocomposites were obtained by coating nano-SiC with Al2O3, where the majority of SiC particles were within the AI2O3 grains. The observation by transmission electron microscopy (TEM) and the analysis by the X-ray photoelectron spectroscopy (XPS) showed thataves propagated towards the intragranular SiC rather than along grain boundaries.
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