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建立了萃取/硝化/石墨炉原子吸收法分析海水中三丁基锡的方法,筛选了最佳的萃取条件、基改剂及石墨炉参数。本方法检出限为016μg/L;相对标准偏差最高不超过4%;回收率为94%~105%。
A method for the extraction of tributyltin in seawater by extraction / nitrification / graphite furnace atomic absorption spectrometry was established. The optimal extraction conditions, base modifiers and graphite furnace parameters were screened. The detection limit of this method was 0.16μg / L; the relative standard deviation was no more than 4%; the recovery was 94% -105%.